DOI: 10.1016/j.marpolbul.2015.03.008
Scopus记录号: 2-s2.0-84929264454
论文题名: Contamination of the southern Baltic Sea waters by the residues of selected pharmaceuticals: Method development and field studies
作者: Borecka M. ; Siedlewicz G. ; Haliński T.P. ; Sikora K. ; Pazdro K. ; Stepnowski P. ; Białk-Bielińska A.
刊名: Marine Pollution Bulletin
ISSN: 0025-326X
EISSN: 1879-3363
出版年: 2015
卷: 94, 期: 2018-01-02 起始页码: 62
结束页码: 71
语种: 英语
英文关键词: Baltic Sea
; LC-MS/MS
; Marine waters contamination
; Matrix effects
; Pharmaceutical residues
; Uncertainty estimation
Scopus关键词: Seawater
; Uncertainty analysis
; Water pollution
; Baltic sea
; LC-MS/MS
; Marine waters
; Matrix effects
; Pharmaceutical residues
; Uncertainty estimation
; Marine pollution
; enrofloxacin
; ibuprofen
; ketoprofen
; naproxen
; oxolinic acid
; sulfadimethoxine
; sulfamerazine
; sulfamethoxazole
; sulfapyridine
; sulfathiazole
; trimethoprim
; drug
; sea water
; water pollutant
; concentration (composition)
; drug
; liquid chromatography
; marine pollution
; mass spectrometry
; seawater
; uncertainty analysis
; Article
; Baltic Sea
; chemometric analysis
; concentration (parameters)
; electrospray mass spectrometry
; extraction
; liquid chromatography
; sea pollution
; solid phase extraction
; tandem mass spectrometry
; validation process
; water analysis
; water sampling
; analysis
; Baltic States
; chemistry
; environmental monitoring
; procedures
; water pollutant
; Atlantic Ocean
; Baltic Sea
; Baltic States
; Environmental Monitoring
; Pharmaceutical Preparations
; Seawater
; Water Pollutants, Chemical
Scopus学科分类: Agricultural and Biological Sciences: Aquatic Science
; Earth and Planetary Sciences: Oceanography
; Environmental Science: Pollution
英文摘要: In this study the occurrence of thirteen pharmaceuticals in seawaters collected from southern Baltic Sea was evaluated for the first time. It was performed by applying newly developed analytical procedure. The method was characterized in terms of its basic validation parameters as well as matrix effects, extraction efficiency and absolute recovery. The results were expressed as result±expanded uncertainty, which was estimated according to the Guide to the Expression of Uncertainty in Measurement. Additionally, in order to verify the influence of variable parameters of the analyzed samples on method performance parameters, chemometric analysis was carried out. The obtained results revealed that residues of pharmaceuticals were present in seawaters at a concentration level of ng L-1. Trimethoprim, sulfamethoxazole and enrofloxacin were most frequently detected compounds. The highest concentration was determined for ketoprofen (135.0 ± 10.9 ng L-1). Marine pollution potential hotspots were found in enclosed or semi-enclosed bodies of water. © 2015 Elsevier Ltd. Citation statistics:
资源类型: 期刊论文
标识符: http://119.78.100.158/handle/2HF3EXSE/86119
Appears in Collections: 过去全球变化的重建 全球变化的国际研究计划
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作者单位: Department of Environmental Analysis, Faculty of Chemistry, University of Gdańsk, ul. Wita Stwosza 63, Gdańsk, Poland; Institute of Oceanology, Polish Academy of Sciences, ul. Powstańców Warszawy 55, Sopot, Poland; Physicochemical Laboratories, Faculty of Chemistry, University of Gdańsk, ul. Wita Stwosza 63, Gdańsk, Poland
Recommended Citation:
Borecka M.,Siedlewicz G.,Haliński T.P.,et al. Contamination of the southern Baltic Sea waters by the residues of selected pharmaceuticals: Method development and field studies[J]. Marine Pollution Bulletin,2015-01-01,94(2018-01-02)